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加拿大帕特森真空干燥機(jī)介紹 |
| 發(fā)布日期：2021-8-17 |
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| 帕特森Industries加拿大“過(guò)程裝備的人”的設(shè)計(jì)，工程和制造許多不同的工業(yè)和化學(xué)流程和應(yīng)用程序的Conaform真空干燥機(jī)。 帕特森Conaform干燥操作的原則基礎(chǔ)上，水或其它揮發(fā)性物質(zhì)的高蒸氣壓的從一個(gè)區(qū)域移動(dòng)到較低壓力區(qū)。這Conaform達(dá)到通過(guò)加熱干燥的材料，可以提高吸收的或游離液體的蒸氣壓，或通過(guò)真空或掃它帶走空氣流通過(guò)的蒸氣的氣體壓力降低。因此，很明顯，Conaform真空干燥系統(tǒng)中提供有效的干燥的基本條件，高效率和均勻的熱傳遞整個(gè)分批..和快速去除蒸汽。帕特森Conaform真空干燥機(jī)可以建在從1立方英尺（0.03立方米）的大小為371立方英尺（10.51立方米）的能力與體直徑從1'6“（0.46米），10英尺6英寸（3.2米）。帕特森Conaform干燥器是完全通過(guò)夾套循環(huán)熱水，油，蒸汽或蒸汽夾套和設(shè)計(jì)。由于Conaform單位轉(zhuǎn)動(dòng)時(shí)，快速和連續(xù)的批次間混合帶來(lái)的每一個(gè)粒子在與被加熱的表面接觸�；旌虾驼郫B用的組合，可以實(shí)現(xiàn)均勻的溫度在整個(gè)批處理，因?yàn)闆](méi)有冷點(diǎn)，防止再縮合，并有助于快速的干燥速度和消除結(jié)塊。在理想的條件下，同時(shí)維持高真空的材料是在運(yùn)動(dòng)中，允許繪圖的水分。帕特森Conaform真空機(jī)是專(zhuān)為快速，高效的干燥各種各樣的化學(xué)品，藥品和食品。其獨(dú)特的雙錐形的回轉(zhuǎn)形狀，保證材料和加熱表面之間的直接接觸。這將導(dǎo)致在高效率和均勻的熱傳遞，并允許高速干燥，干燥溫度不提高被加工的材料的危險(xiǎn)點(diǎn)。的PATTERSON Conaform是非常溫和的行動(dòng)。移動(dòng)部件的情況下，保證對(duì)解體的鋒利邊緣或拐角的晶體或磨損。由于是密封的烘干機(jī)，操作無(wú)粉塵。這意味著，沒(méi)有重大損失和沒(méi)有污染的氣氛。帕特森Conaform被設(shè)計(jì)為沒(méi)有電容器或其他輔助設(shè)備中使用的許多材料的干燥。 ，通常一個(gè)Conaform將取代整個(gè)系列的托盤(pán)微波爐。如冷凝器，傾析器等，是必需的，他們可以適當(dāng)大小的為每Conaform的機(jī)。帕特森Conaform是提供一個(gè)特殊的分散機(jī)制稱(chēng)為作為Conagrator，材料傾向于在干燥過(guò)程中形成硬塊。使用一個(gè)Conagrator有助于實(shí)現(xiàn)高的干燥速率，即使當(dāng)處理結(jié)晶材料。應(yīng)用范圍：帕特森Conaform真空干燥機(jī)在除了干燥功能，也可以用于混合，加熱，冷卻和用于液體或氣體的添加劑等功能。它們被用于廣泛的食品物質(zhì)，藥品和化學(xué)品干燥。帕特森Conaform真空機(jī)已經(jīng)使用的進(jìn)程，需要預(yù)混合的液體添加劑，此外，加熱的內(nèi)容帶出了反應(yīng)，清除多余的水分，^后冷卻批次的產(chǎn)品。設(shè)計(jì)特點(diǎn)：室內(nèi)清潔 - 易于保持清潔 Conaform干燥器的內(nèi)部?jī)H由光滑的側(cè)壁，通過(guò)它的熱量被傳遞到產(chǎn)品。干燥室的獨(dú)特的雙圓錐形狀實(shí)現(xiàn)混合和摻合的行動(dòng)。缸和截錐體的相交是鈍角，所以沒(méi)有材料被困住。有沒(méi)有內(nèi)部的刮削器，犁，勺子或葉片捕獲和材料，或防止干燥均勻。Conaform可以很容易地清洗快速變化的產(chǎn)品或顏色，保持^小的過(guò)程。此功能使一個(gè)干燥器沒(méi)有交叉污染的產(chǎn)品可用于許多不同的試劑級(jí)化學(xué)品的^高純度。致密真空密封 Conaform有一個(gè)填料函，在入口處的蒸汽管道。易于維護(hù)，高效真空，真空能力過(guò)剩并不需要提供的泄漏。其他固定筒干燥機(jī)的類(lèi)型與水平軸攪拌器需要兩個(gè)填料箱，或批次的軸承內(nèi)部。軸承OUT的批處理 所有軸承的Conaform安裝在干燥室的外面。有沒(méi)有潤(rùn)滑劑的產(chǎn)品污染的可能性。真空密封無(wú)塵排氣閥 為了保持^高的產(chǎn)品純度和無(wú)塵操作，Conaform干燥器配有特別設(shè)計(jì)的真空密封的排出閥。該閥是一個(gè)光滑的板坐在與蝸桿驅(qū)動(dòng)器。有一點(diǎn)力氣堅(jiān)決座閥。通暢的流動(dòng)，類(lèi)似一個(gè)閘閥，它完全打開(kāi)，但沒(méi)有任何凹槽或通道捕獲材料。圍繞閥的輪輞提供的座椅的安裝套筒，所以也沒(méi)有損失的產(chǎn)品和沒(méi)有在放電過(guò)程中的污染。無(wú)破損或磨損的晶體 Conaform機(jī)是溫和的行動(dòng)。整個(gè)沒(méi)有移動(dòng)部分內(nèi)的Conaform確保打擊解體的鋒利邊緣或拐角的晶體或磨損。這是一個(gè)無(wú)灰塵的^終產(chǎn)物所需的特殊的優(yōu)勢(shì)。無(wú)結(jié)塊 - NO污染 由于Conaform旋轉(zhuǎn)，和真空吸走水分，顆粒不斷地改變自己的立場(chǎng)。沒(méi)有結(jié)塊，或污染的Conaform，在其他類(lèi)型的干燥器。晶體板或拉長(zhǎng)身材不包，但采取隨機(jī)的方向，開(kāi)放空間的蒸氣逃脫。溶劑回收 帕特森Conaform干燥器干燥價(jià)值高的材料是特別有用的。從在干燥的材料中提取的溶劑或液體可以回收所使用的冷凝器。輔助設(shè)備，如冷凝器，傾析器，等等，可以提供與任何規(guī)模的Conaform干燥器�？梢允褂貌粠Ю淠� Conaform可以用于多種材料的干燥沒(méi)有電容器或其他設(shè)備。優(yōu)于盤(pán)架干燥 conaform真空干燥是優(yōu)異的許多方法來(lái)托盤(pán)干燥。在盤(pán)架干燥，循環(huán)空氣預(yù)熱的材料和刪除只從表面層中的水分。所有的蒸汽沒(méi)有上升到表面，但移動(dòng)到的地方的^低蒸氣壓力 - 通常是中心的批次，由于惡劣的熱滲透。這里，它被冷凝，或者被重吸收引起結(jié)塊。通過(guò)熱傳導(dǎo)的材料的多孔床總是慢，和輻射轉(zhuǎn)移是眾所周知的低效率的，在低溫下，與真空干燥。同時(shí)在真空條件下干燥Conaform原則消除這些不足之處，并提供一致的產(chǎn)品每次。單位可以單獨(dú)設(shè)計(jì)，以客戶的材料規(guī)格和工藝參數(shù)。完成的Conaform的規(guī)格表，并通過(guò)電子郵件或傳真提交帕特森的報(bào)價(jià)。 完成PATTERSON真空干燥系統(tǒng)由以下幾部分組成：（A）PATTERSON＃5 1'0“體直徑Conaform真空式干燥機(jī) - 雙圓錐機(jī)，^大工作容積0.32立方英尺，額定工作容量：0.32立方英尺，身體總體積：0.49立方英尺，約。換熱面積：2.9平方尺接觸的所有部件：316不銹鋼，夾克產(chǎn)品支持的立場(chǎng)和基地304不銹鋼。設(shè)計(jì)條件：吹風(fēng)機(jī)本體：100（212），全真空外套：25 psig至100（212）一致內(nèi)部全真空，內(nèi)表面拋光，電拋光180號(hào)，體絕緣，SS304護(hù)套覆蓋，完整的HP不可分割的體速度：10 rpm的電機(jī)減速機(jī)，齒輪。應(yīng)用領(lǐng)域：癌癥藥物的研究/制造（B）1.25 HP TEFC電機(jī)與單級(jí)旋片式真空泵真空系統(tǒng)，泄壓閥，進(jìn)口止回閥。（C）（1）只有4.5千瓦熱水/冷卻循環(huán)水系統(tǒng)與電子溫度和過(guò)程控制器，具有數(shù)字通信接口，主控制面板。（D）控制系統(tǒng)的面板。自動(dòng)基于微型處理器的控制系統(tǒng)將保持設(shè)定溫度的加熱周期的長(zhǎng)度上。在加熱周期的時(shí)間和其他參數(shù)將被設(shè)置在開(kāi)始的過(guò)程周期。溫度和真空度，將被記錄的周期的長(zhǎng)度上，并可以被下載到一個(gè)標(biāo)準(zhǔn)的PC擴(kuò)散片材或其他格式。該系統(tǒng)會(huì)自動(dòng)將控制的序列過(guò)程循環(huán)，烘干機(jī)旋轉(zhuǎn)，熱真空，熱切斷周期結(jié)束時(shí)。該控制系統(tǒng)包括：主輸入開(kāi)關(guān)斷開(kāi) 安裝在面板上的人機(jī)界面觸摸屏PLC 8“標(biāo)準(zhǔn)彩色面板，640×480像素的分辨率與相應(yīng)的圖形顯示控制所有設(shè)備，如烘干機(jī)，真空系統(tǒng)和加熱器。 數(shù)字溫度指示器 真空泵控制 數(shù)字真空指示器 機(jī)控制 電阻式模擬觸摸屏作為人機(jī)界面 RS232通訊端口和RS485連接到PC的數(shù)據(jù)采集等 （E）系統(tǒng)的所有組件連接到控制面板間的連接管道是撬裝 驅(qū)動(dòng)系統(tǒng)側(cè)視圖 非系統(tǒng)驅(qū)動(dòng)器的側(cè)視圖 熱水/冷卻循環(huán)水系統(tǒng)控制面板的前視圖 關(guān)閉真空泵 主屏幕 機(jī)控制 過(guò)程控制 真空控制 設(shè)定點(diǎn)的溫度 增量小時(shí) 容器的溫度 溫度監(jiān)控器 溫度監(jiān)控器 調(diào)節(jié)對(duì)比度 報(bào)警歷史記錄 控制系統(tǒng) 請(qǐng)注意：帕特森的內(nèi)部專(zhuān)業(yè)知識(shí)，設(shè)計(jì)和提供我們所有的工藝設(shè)備的操作控制系統(tǒng)，無(wú)論是一個(gè)簡(jiǎn)單的開(kāi)始/停止周期時(shí)間或執(zhí)行復(fù)雜的多階段系統(tǒng)配方或公式，并與現(xiàn)有的工廠控制系統(tǒng)。關(guān)閉控制箱，起動(dòng)/停止，點(diǎn)動(dòng)/運(yùn)行和0-12小時(shí)定時(shí)器。 包括HMI觸摸屏控制面板概述。 特寫(xiě)與PLC和變頻電機(jī)控制器的控制面板內(nèi)的。PATTERSON Industries Canada "The Process Equipment People" designs, engineers and manufactures Conaform Vacuum Dryers for many different industrial and chemical processes and applications. The PATTERSON Conaform drying operations are based on the principle that water or other volatile material moves from a zone of high vapor pressure to a zone of lower pressure. The Conaform attains this by warming the material to be dried to raise the vapor pressure of the absorbed or free liquid, or by decreasing the vapor pressure of the gas by vacuum or by sweeping it away with an air current. Thus, it is apparent that the Conaform Vacuum Dryer System provides the essential conditions for effective drying, efficient and uniform heat transfer throughout the batch .. and rapid removal of vapor.PATTERSON Conaform Vacuum Dryers can be built in sizes from 1 cubic foot (0.03 cu. m) to 371 cubic feet (10.51 cu. m) capacity with body diameters from 1' 6" (.46 m) to 10' 6" (3.2 m).PATTERSON Conaform Dryers are completely jacketed and designed for circulating hot water, oil, steam or vapors through the jacket. As the Conaform Unit rotates, the rapid and continuous inter-mixing of the batch brings every particle in contact with the heated surface. The combination of blending and interfolding helps achieve uniform temperature throughout the batch, prevents re-condensation since there are no cold spots, and contributes to rapid drying speed and the elimination of caking. Maintaining a high vacuum while the material is in motion permits the drawing off of moisture under ideal conditions.The PATTERSON Conaform Vacuum Dryer is designed for fast, efficient drying of a wide variety of chemicals, pharmaceuticals and food products. Its unique double cone rotating shape assures direct contact between the material and the heated surfaces. This results in efficient and uniform heat transfer and permits high speed drying without raising the drying temperature to the danger point of the material being processed.The PATTERSON Conaform is exceptionally gentle in action. The absence of moving parts assures against disintegration of crystals or abrasion of sharp edges or corners. Since the dryer is hermetically sealed, operations are dust -free. This means no material loss and no contamination of the atmosphere.The PATTERSON Conaform is designed for use in the drying of many materials without condensers or other auxiliary equipment. One Conaform will usually replace an entire series of tray ovens. Where condensers, decanters, etc., are required, they can be properly sized for every Conaform Dryer.The PATTERSON Conaform is available with a special dispersing mechanism known as the Conagrator, for materials that tend to form lumps in the drying process. The use of a Conagrator helps achieve high drying rates even when handling crystalline material.Applications:The PATTERSON Conaform Vacuum Dryer in addition to the drying feature can also be used for such functions as blending, heating, cooling and for liquid or gaseous additives. They are used for drying a wide range of food substances, pharmaceuticals and chemicals.The PATTERSON Conaform Vacuum Dryer has uses in processes requiring pre-blending, addition of liquid additives, heating the contents to bring out a reaction, removal of excess moisture and finally cooling of the batch of product.Design Features:A CLEAN INTERIOR - EASY TO KEEP CLEAN The interior of the Conaform Dryer consists only of the smooth sidewalls, through which the heat is transferred to the product. The unique double-cone shape of the drying compartment achieves the mixing and blending action. Intersections of cylinder and truncated cones are obtuse angles, so no material is trapped. There are no internal scrapers, plows, scoops or vanes to trap and hold material or prevent uniform drying.The Conaform can be easily cleaned for quick change of products or colors, with minimum process hold-up. This feature enables one Dryer to be used for many different reagent-grade chemicals of highest purity without cross contamination of products.TIGHT VACUUM SEAL The Conaform has one stuffing box-at the entrance of the vapor pipe. A highly efficient vacuum is easily maintained, as excess vacuum capacity is not required to provide for leakage. Other dryers of the stationary cylinder type with horizontal shaft agitator require two stuffing boxes, or a bearing inside of the batch.BEARINGS OUT OF THE BATCH All bearings of the Conaform are installed outside of the drying compartment. There is no possibility of product contamination from lubricants.VACUUM-TIGHT DUSTLESS DISCHARGE VALVE To maintain highest product purity and dust-free operation, the Conaform Dryer is fitted with a specially designed vacuum-tight discharge valve. The valve is a smooth plate seated with a worm drive. There is little effort required to firmly seat the valve. It opens fully, for unobstructed flow, similar to a gate valve, but has no grooves or channels to trap material. The rim around the valve provides a seat for attaching a sleeve, so there is no loss of product and no contamination during discharge.NO BREAKAGE OR ABRASION OF CRYSTALS The Conaform Dryer is gentle in action. The entire absence of moving parts within the Conaform ensures against disintegration of crystals or abrasion of sharp edges or corners. This is of special advantage where a dust-free final product is desired.NO CAKING - NO CONTAMINATION As the Conaform rotates, and the vacuum draws off moisture, the particles constantly change their position. There is no caking, or contamination in the Conaform, as in dryers of other types. Crystals of plate or elongated shape do not pack but take random orientation, leaving open space for vapor to escape.FOR SOLVENT RECOVERY The PATTERSON Conaform Dryer is particularly useful for drying materials of high value. Solvents or liquids extracted from the materials being dried may be recovered by the use of condensers. Auxiliary equipment, such as condensers, decanters, etc., can be supplied with any size Conaform Dryer.MAY BE USED WITHOUT CONDENSER The Conaform can be used for drying many materials without condensers or other equipment.SUPERIOR TO TRAY DRYING Conaform vacuum drying is superior in many ways to tray drying. In tray drying, the circulating air warms the material and removes moisture from the surface layer only. All vapors do not rise to the surface but move to the place of lowest vapor pressure - often the center of the batch, because of poor heat penetration. Here it is condensed or is reabsorbed to cause caking. Heat conduction through a porous bed of material is always slow, and transfer by radiation is notoriously inefficient at the low temperature associated with vacuum drying. The Conaform? principle of simultaneous drying under a vacuum eliminates these deficiencies and delivers a consistent product everytime.Units can be individually designed to customer's material specifications and process parameters. Complete the Conaform Specification Sheet and submit by e-mail or fax to PATTERSON for quotation. Complete PATTERSON Vacuum Drying System consisting of the following components:(A) PATTERSON Model #5, 1'0" body diameter Conaform Vacuum Dryer-Double Cone Dryer, Maximum Operating Capacity 0.32 cu.ft, Nominal Working Capacity: .32 cu.ft, Total Body Volume: 0.49 cu.ft, Approx. Heat Transfer Area: 2.9 sq. ft. All parts contacting product 316 stainless, Jacket support stands and base 304 Stainless Steel. Design Conditions: Dryer Body: Full Vacuum to 100 (212), Jacket: 25 psig to 100 (212) coincident with Internal Full Vacuum, Internal surfaces polished to 180 grit followed by electro-polishing, body insulated and covered with SS304 sheathing, complete with HP integral gear motor reducer, Body Speed: 10 rpms.Application: Cancer Drug Research/Manufacturing(B) Vacuum System with single stage Rotary Vane Vacuum Pump with 1.25 HP TEFC motor, bleed valve and inlet check valve.(C) One (1) only 4.5 kW Hot Water/Cooling Circulating System with electronic temperature and process controller with digital communication interface to main control panel.(D) Control System with Panel. The automatic micro processor based control system will maintain the set temperature over the length of the heating cycle. The time for the heating cycle and other parameters will be set at the beginning of the process cycle. Temperature and vacuum will be recorded over the length of the cycle and can be downloaded to a standard PC spread sheet or other format. The system will automatically control the sequence for process cycle, Dryer rotation, heat, vacuum, cut off of heat at end of cycle.The Control System includes:Main input disconnect switch Panel-mounted HMI Touch screen PLC 8" Standard colour panel, 640 x 480 pixel resolution with appropriate graphics showing control of all devices such as Dryer, Vacuum System, and Heater. Digital Temperature Indicator Vacuum Pump Controls Digital Vacuum Indicator Dryer Controls Resistive Analog Touchscreen as HMI interface RS232 communications Port and RS485 for connection to PC for data acquisition etc. included (E) System is skid mounted with all components wired to the control panel and inter-connecting piping Drive side view of System Non Drive Side view of System Front view of Control Panel with Hot Water/Cooling Circulating System Close up view of Vacuum Pump Main Screen Dryer Control Process Control Vacuum Control Set point Temperature Increment Hour Vessel Temperature Temperature Monitor Temperature Monitor Adjust Contrast Alarm History Control Systems Please note: PATTERSON has in-house expertise to design and supply operating control systems for all of our process equipment, whether it is a simple start/stop with cycle time or complex multi-stage systems executing recipes or formulas and communicating with existing plant control systems.Close up of Control Box with stop/start, jog/run and 0-12 hr timer. Control Panel Overview including HMI Touch Screen. Close-up of Inside of Control Panel with PLC and Variable Frequency Motor Controllers. |
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在制藥領(lǐng)域，干燥設(shè)備是必不可少的裝備，隨著行業(yè)要求的提升及技術(shù)的發(fā)展，干燥設(shè)備的種類(lèi)不斷增多，真空干燥設(shè)備憑借其優(yōu)勢(shì)迅速占領(lǐng)了藥機(jī)市場(chǎng)。 真空干燥機(jī)，在低壓下干燥時(shí)氧含量低，能防止被干燥物料氧化變質(zhì)，可干燥易燃易爆的危險(xiǎn)品；可在低溫下使物料中的水分汽化，易于干燥熱敏性物料；能回收被干燥物料中的貴重和 確定哪種真空干燥器適合特定應(yīng)用，部分取決于了解固體材料的水分含量；此外，了解材料的顆粒特性非常重要，因?yàn)檫@些特性可能會(huì)在不同的濕度水平下以不可預(yù)期的方式變化。例如，含有40％水分的濾餅可以比含有15％水分的濾餅更好地流動(dòng)。仔細(xì)評(píng)估影響選擇的許多可能因素將有助于減少選項(xiàng)的數(shù)量。真空干燥機(jī)中的雙錐回轉(zhuǎn)真空干燥機(jī)為雙錐形真空條件下旋轉(zhuǎn)內(nèi)桶，罐，向夾套內(nèi)通入罐壁和濕物料接觸，濕料蒸汽或熱水加熱，加熱后的水吸收熱量蒸發(fā)汽，真空泵真空排氣管被泵出。由于內(nèi)箱的是在真空狀態(tài)下，并且該罐體旋轉(zhuǎn)材料連續(xù)地向上和轉(zhuǎn)動(dòng)，從而加快該材料的干燥速度，提高干燥效率，達(dá)到均勻干燥的目的。雙錐回轉(zhuǎn)真空干 通常建議對(duì)大量潮濕或潮濕的材料進(jìn)行真空冷凍干燥，進(jìn)入真空冷凍干燥室時(shí)材料必須處于冷凍狀態(tài)，并在整個(gè)干燥過(guò)程中保持冷凍狀態(tài)。在低于冰點(diǎn)的溫度下將物品置于高真空中，同時(shí)施加受控?zé)崃康难h(huán)；該過(guò)程使冷凍水升華為蒸汽而不通過(guò)液相-有利于使可溶性介質(zhì)的羽化和滲出小化。 &em真空干燥機(jī)用于脫水的材料，這需要將其干燥到水分含量非常低，達(dá)到很高的水平，在嚴(yán)密控制的方式干燥，從而保持產(chǎn)品的完整性。真空干燥過(guò)程中經(jīng)常被用來(lái)干燥微妙的物料，如食品，藥品和生物樣品。它可以被用來(lái)減少產(chǎn)品損失，否則可能導(dǎo)致大氣污染物。真空干燥，也可以是一種高效的方法，為保存和長(zhǎng)期存儲(chǔ)的有害材料。MEC
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